Chemical and Reagents:
- GC Grade Nitrogen, hydrogen and air.
- Propylene glycol (CAS 57-55-6), Reagent grade
- Methanol (CAS 67-56-1)
- Sample
Instruments and Apparatus:
- 4ml Vials with Teflon-lined caps
- Gas Chromatograph equipped with Flame Ionization Detector (FID)
- Electronic integrator
- 10µl syringe
- Pipettes
- Volumetric flasks
- Electronic Balance
- GC Grade Nitrogen, hydrogen and air.
- Propylene glycol (CAS 57-55-6), Reagent grade
- Methanol (CAS 67-56-1)
- Sample
Instruments and Apparatus:
- 4ml Vials with Teflon-lined caps
- Gas Chromatograph equipped with Flame Ionization Detector (FID)
- Electronic integrator
- 10µl syringe
- Pipettes
- Volumetric flasks
- Electronic Balance
Gas Chromatography Conditions:
Injection size:
|
1 µL
|
Flow rates
(mL/min)
|
|
Nitrogen
(make-up):
|
30
|
Hydrogen
(carrier):
|
2
|
Hydrogen
(detector):
|
40
|
Air:
|
420
|
Temperatures (°C)
|
|
Injector:
|
200
|
Detector:
|
275
|
Column:
|
40 isothermal
|
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